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We studied Fe3P Impurity Phase in LiFePO4. By using X-Ray Diffraction the presence of ferromagnetic Fe3P crystallites was revealed; by Small-Angle X-ray Scattering (SAXS),the size of magnetic-nuclear contrasting regions was detected. This study employs advanced tool for the determination of the impurity. The content of this work clarify the novelty and the stated results and also has detailed comparison.