Synthesis of Bis- and Tris-Organophosphorus Substituted Amines and Amino Acids with PCH2N Fragmentsстатья
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Аннотация:The aminomethylation of the derivatives of trivalent organophosphorus acids, containing PH and POSiMe3 fragments with various bis- and tris(alkoxymethyl)amines and bis(alkoxymethyl)amino acids, is proposed as a convenient method for the synthesis of new bis- and trisphosphorylated amines and amino acids as well as their derivatives with four and five coordinated phosphorus. Also the three-components systems of phosphorous acid, paraformaldehyde, and amines are thoroughly investigated via the treatment of reaction mixtures with bis (trimethylsilyl)amine. (C) 2010 Wiley Periodicals, Inc. Heteroatom Chem 21:430-440, 2010; View this article online at wileyonlinelibrary.com. DOI 10.1002/hc.20616